Habka isku dhafka ah ee tantalum pentachloride

Habka isku dhafka ah eetantalum pentachlorideInta badan waxaa ku jira tillaabooyinka soo socda:
1. Diyaarinta alaabta ceeriin
Diyaarso nadiif sarebiraha tantalumiyo koloriin-nadiifin sare leh ama hydrogen chloride (HCl) oo ah alaab cayriin ah. daahirnimada eebiraha tantalumwaxay saameyn weyn ku leedahay nadiifnimada alaabta ugu dambeysa.
2. falcelinta koloriin
Habka koloriinta tooska ah:Tantalum birtawaa la jarjaray ama la budada ah, ka dibna la dhex geliyaa qulqulka gaaska koloriin si loogu sameeyo falcelinta koloriinta ee heerkulka u dhexeeya 170-250. Gaaska Chlorine wuxuu la falgalaa tantalum si uu u soo saarotantalum pentachloride. Dareen-celintan sidoo kale waxaa lagu samayn karaa iyadoo la isticmaalayo HCl, laakiin waxay u baahan tahay in lagu sameeyo heerkul sare (sida 400).
Habka koloriinaynta aan tooska ahayn: Tantalum pentachloride sidoo kale waxaa lagu heli karaa ka falcelinta tantalum pentoxide leh thionyl chloride (SOCl2) at 240 ° C. Isla'egta falcelinta waa: Ta2O5+5 SOCl2 → 2 TaCl5+5 SO2.
3. Kala saarida iyo nadiifinta
Qabooji gaaska ay soo saarto falcelinta koloriinaynta si aad isugu ururiso dareere.
Kala saar oo nadiifi dareerahatantalum pentachloridewasakhda ka timaada. Caadi ahaan, distillation iyo habab kale ayaa loo isticmaalaa in lagu kala saaro wasakhaha kala duwan iyadoo lagu saleynayo farqiga dhibcaha karkarinta. Tallaabadan ayaa fure u ah xaqiijinta nadiifnimadatantalum pentachloride.
4. Daawaynta qalajinta
Qalaji kuwa kala soocay oo la nadiifiyeytantalum pentachloridesi looga saaro qoyaanka dusha sare iyo wasakhda. Daaweynta qallajinta ayaa muhiim u ah ilaalinta xasiloonida iyo nadiifnimada tantalum pentachloride.